溶剂热法合成Fe_3O<sub>4</sub>八面体微晶及表征

阿布都赛买提·塔吉; 彭登峰; 拜山·沙德克

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溶剂热法合成Fe_3O₄八面体微晶及表征

工程技术 | 更新时间：2026-01-21

- 溶剂热法合成Fe_3O₄八面体微晶及表征
- 溶剂热法合成Fe_3O₄八面体微晶及表征
- 新疆大学学报（自然科学版中英文） 2011年28卷第1期页码：71-75
- 作者机构：
  
  1. 新疆大学物理科学与技术学院
  2. 同济大学功能材料研究所
- 作者简介：
- 基金信息：
  
  国家自然科学基金资助项目(50661005);国家教育部留学回国人员科研启动基金资助项目(030205)
- DOI：
  中图分类号： TB383.1
- 纸质出版：2011
- 稿件说明：
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[1]阿布都赛买提·塔吉,彭登峰,拜山·沙德克.溶剂热法合成Fe_3O_4八面体微晶及表征[J].新疆大学学报(自然科学版),2011,28(01):71-75.

阿布都赛买提·塔吉, 彭登峰, 拜山·沙德克. 溶剂热法合成Fe_3O₄八面体微晶及表征[J]. Journal of Xinjiang University (Natural Science Edition in Chinese and English), 2011, 28(1): 71-75.
[1]阿布都赛买提·塔吉,彭登峰,拜山·沙德克.溶剂热法合成Fe_3O_4八面体微晶及表征[J].新疆大学学报(自然科学版),2011,28(01):71-75. DOI：

阿布都赛买提·塔吉, 彭登峰, 拜山·沙德克. 溶剂热法合成Fe_3O₄八面体微晶及表征[J]. Journal of Xinjiang University (Natural Science Edition in Chinese and English), 2011, 28(1): 71-75. DOI：

摘要

以氯化亚铁作为铁源

在碱性条件下通过混合溶剂热法合成了大尺寸Fe3O4八面体微晶.用X射线衍射仪(XRD)

能量分散谱(EDS)

扫描电子显微镜(SEM)对所得样品进行了物相

成分和形貌表征

磁性用振动样品磁强计(VSM)测试.结果显示

我们样品是纯立方相

形貌完整

高结晶度Fe3O4八面体.还发现

在混合溶液中随着乙二醇和水合肼体积比在一定范围内增大时

所得八面体尺寸也显出随之增大的趋势;样品具有跟块体接近的磁化强度Ms和相对较小的矫顽力Hc.

Abstract

Using ferrous chloride as iron sources

octahedral magnetite microcrystals with larger size were synthesized by the means of a mixed solvothermal method in alkaline condition.The chemical composi-tions

morphologies were characterized by XRD

EDS

SEM measurements and magnetic measurement was conducted by Vibrating Sample Magnetometer(VSM).It is showed that our sample are pure cubic phase magnetite octahedrons with uniform morphology and high crystallinity.The size of magnetite octahedrons tended to largen as the volume ratio of ethylene glycol to hydrazine hydrate increased to particular range.The sample possessed saturation magnetization and coercive field that close to and much lower than that of the bulk respectively.

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溶剂热法合成Fe_3O4八面体微晶及表征

溶剂热法合成Fe_3O4八面体微晶及表征

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摘要

Abstract

关键词

Keywords

references

溶剂热法合成Fe_3O₄八面体微晶及表征

溶剂热法合成Fe_3O₄八面体微晶及表征