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新疆大学理化测试中心
Published:2011
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[1]唐军,王强,白希,等.超声辅助提取伽师瓜籽油工艺及其脂肪酸成分研究[J].新疆大学学报(自然科学版),2011,28(02):226-229+233.
唐军, 王强, 白希, et al. 超声辅助提取伽师瓜籽油工艺及其脂肪酸成分研究[J]. Journal of Xinjiang University (Natural Science Edition in Chinese and English), 2011, 28(2): 226-229.
采用超声辅助提取伽师瓜籽油
筛选了提取伽师瓜籽油的理想溶剂
通过正交试验考察了提取温度、提取时间、料液比对伽师瓜籽油得率的影响.结果表明
石油醚为提取伽师瓜籽油的理想溶剂;三个因素对伽师瓜籽油得率的影响大小依次为:超声温度>料液比>超声时间;优化的提取参数为:超声温度60°C、料液比1:6(W/V)、提取时间20 min
此条件下伽师瓜籽油的得率达到36.97%.利用气相色谱—质谱联用(GC/MS)技术对伽师瓜籽的脂肪酸组成进行了分析
发现甜瓜籽油中共有11种脂肪酸
脂肪酸组成为棕榈酸
亚油酸
油酸
硬脂酸
十八碳烯酸
蓖麻醇酸
11-二十碳烯酸
花生酸
榆树酸
以及山嵛酸.从相对含量看
亚油酸含量最高.
Cucurbitaceae melo var.saccharinus Naud.seed oil was extracted by ultrasound method in this study.Effects of extraction solvent
extraction temperature
and extraction time
ratio of material to liquid on oil yield were investigated by orthogonal design.The results showed that the optimal extrac-tion solvent is petroleum ether.The significance sequence of other three factors affecting oil yield is as follows:extraction temperature > ratio of material to liquid > extraction temperature
and their optimumlevels are 60°C
1:6(m/V)
20min respectively.Under these conditions
the oil yield reaches 36.97 %.GC/MS analysis was used to determine the fatty acid composition of the Cucurbitaceae melo var.saccharinus Naud.seed oil.It was found that the main fatty acids in the oil are palmitic acid
linoleic acid
oleic acid
stearic acid
octadecenic acid
methyl ricinoleate
11-eicosenoic acid
eicosanoic acid
docosanoic acid and tetracosanoic acid.The relative content of linoleic acid is the highest.
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